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Selective INEPT, a new technique for the 13 C NMR assignment of methylene carbons with non‐equivalent protons, and its application to the analysis of the 13 C NMR spectrum of monensin
Author(s) -
Furihata Kazuo,
Seto Haruo,
Ohuchi Muneki,
Otake Noboru
Publication year - 1983
Publication title -
organic magnetic resonance
Language(s) - English
Resource type - Journals
SCImago Journal Rank - 0.483
H-Index - 72
eISSN - 1097-458X
pISSN - 0030-4921
DOI - 10.1002/omr.1270211007
Subject(s) - methylene , proton , chemistry , carbon 13 nmr satellite , proton nmr , analytical chemistry (journal) , nuclear magnetic resonance spectroscopy , fluorine 19 nmr , physics , stereochemistry , nuclear physics , organic chemistry
A new method based on the combination of selective proton decoupling and INEPT is explained in detail. This technique, named selective INEPT (SEL‐INEPT), is a useful and sensitive method for the 13 C NMR assignment of methylene carbons with non‐equivalent protons. The 13 C NMR spectrum of monensin has been analysed by the application of this technique.