Spectral editing for  13 C NMR signals of deuterated compounds | Zendy

Wesener Joachim R. | Zendy; Günther Harald | Zendy

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Spectral editing for 13 C NMR signals of deuterated compounds

Author(s) -

Wesener Joachim R.,

Günther Harald

Publication year - 1983

Publication title -

organic magnetic resonance

Language(s) - English

Resource type - Journals

SCImago Journal Rank - 0.483

H-Index - 72

eISSN - 1097-458X

pISSN - 0030-4921

DOI - 10.1002/omr.1270210707

Subject(s) - deuterium , decoupling (probability) , spectral analysis , chemistry , nuclear magnetic resonance , physics , stereochemistry , nuclear physics , engineering , quantum mechanics , spectroscopy , control engineering

J‐modulation of 13 C spin echo signals is used to develop a strategy for the analysis of deuterated compounds. On the basis of 1 J ( 13 C 2 H) and an experimental set‐up that allows both 2 H and 1 H decoupling, 13 C subspectra for various groups can be produced. The application of difference methods facilitates the analysis and, finally, leads to the identification of CD, CD 2 , CD 3 , CHD, CHD 2 and CH 2 D groups.

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