1 H,  13 C and  31 P NMR spectral analysis of monoalkyl (α‐anilinobenzyl)phosphonates and their dipalladium(II) metallocyclic complexes | Zendy

TušekBožić Ljerka | Zendy; Lyčka Antonin | Zendy

Premium

1 H, 13 C and 31 P NMR spectral analysis of monoalkyl (α‐anilinobenzyl)phosphonates and their dipalladium(II) metallocyclic complexes

Author(s) -

TušekBožić Ljerka,

Lyčka Antonin

Publication year - 2002

Publication title -

magnetic resonance in chemistry

Language(s) - English

Resource type - Journals

SCImago Journal Rank - 0.483

H-Index - 72

eISSN - 1097-458X

pISSN - 0749-1581

DOI - 10.1002/mrc.982

Subject(s) - chemistry , heteronuclear molecule , carbon 13 nmr , stereochemistry , palladium , nuclear magnetic resonance spectroscopy , organic chemistry , catalysis

A 1 H, 13 C and 31 P NMR study of monoethyl (HL1) and monobutyl (HL2) esters of (α‐anilinobenzyl)phosphonic acid and their metallocyclic dipalladium complexes (Pd 2 L 4 ,L = L1, L2) in DMSO‐ d 6 was performed, based on 1D and 2D homo‐ and heteronuclear experiments including 1 H, 13 C, 31 P,APT, 1 H– 1 H COSY, 1 H– 13 C COSY, gs‐HMQC and gs‐HMBC NMR techniques. The results obtained are discussed with respect to those for some palladium(II) complexes reported for various anilinobenzylphosphonate derivatives. Copyright © 2002 John Wiley & Sons, Ltd.

This content is not available in your region!

Continue researching here.

Having issues? You can contact us here

Accelerating Research