Premium
Isolation and characterization of roridin E
Author(s) -
Ridge Clark D.,
Mazzola Eugene P.,
Coles Martyn P.,
Hinkley Simon F. R.
Publication year - 2017
Publication title -
magnetic resonance in chemistry
Language(s) - English
Resource type - Journals
SCImago Journal Rank - 0.483
H-Index - 72
eISSN - 1097-458X
pISSN - 0749-1581
DOI - 10.1002/mrc.4539
Subject(s) - chemistry , isolation (microbiology) , characterization (materials science) , stereochemistry , nanotechnology , microbiology and biotechnology , materials science , biology
Abstract The commonly occurring, high‐cytotoxicity macrolide roridin E has been re‐isolated from Stachybotrys chartarum and characterized by 1‐D and 2‐D NMR spectroscopy. Assignment of the spectral data for roridin E revealed differences from the accepted literature, and spectra are reported herein to aid in future identification. For the first time confirmation of structure was provided by a crystallographic solution for roridin E. Copyright © 2016 John Wiley & Sons, Ltd.