Complete NMR assignment of 3, 4‐ seco ‐lup‐20(29)‐en‐3‐oic acid from  Decatropis bicolor | Zendy

Ríos María Yolanda | Zendy; RamírezCisneros M. Ángeles | Zendy; LeónRivera Ismael | Zendy; EstradaSoto Samuel | Zendy; NavarreteVázquez Gabriel | Zendy; AguilarGuadarrama A. Berenice | Zendy

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Complete NMR assignment of 3, 4‐ seco ‐lup‐20(29)‐en‐3‐oic acid from Decatropis bicolor

Author(s) -

Ríos María Yolanda,

RamírezCisneros M. Ángeles,

LeónRivera Ismael,

EstradaSoto Samuel,

NavarreteVázquez Gabriel,

AguilarGuadarrama A. Berenice

Publication year - 2012

Publication title -

magnetic resonance in chemistry

Language(s) - English

Resource type - Journals

SCImago Journal Rank - 0.483

H-Index - 72

eISSN - 1097-458X

pISSN - 0749-1581

DOI - 10.1002/mrc.2875

Subject(s) - chemistry , two dimensional nuclear magnetic resonance spectroscopy , stereochemistry , heteronuclear single quantum coherence spectroscopy , carbon 13 nmr , rutaceae , botany , biology

Complete 1 H and 13 C NMR chemical shift assignments for 3,4‐ seco ‐lup‐20(29)‐en‐3‐oic acid ( 1 ) have been established by means of two‐dimensional COSY, HSQC, HMBC and NOESY spectroscopic experiments as well as by analysis of MS data. Compound 1 was isolated from Decatropis bicolor (Zucc.) Radlk. (Rutaceae) in addition to six coumarins and one alkaloid of known structure. Copyright © 2012 John Wiley & Sons, Ltd.

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