Dipolar recoupling of  I  = 1/2,  S  = 3/2 spin pairs with SEDOR for static and spinning samples | Zendy

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Dipolar recoupling of I = 1/2, S = 3/2 spin pairs with SEDOR for static and spinning samples

Author(s) -

Gullion Terry

Publication year - 2007

Publication title -

magnetic resonance in chemistry

Language(s) - English

Resource type - Journals

SCImago Journal Rank - 0.483

H-Index - 72

eISSN - 1097-458X

pISSN - 0749-1581

DOI - 10.1002/mrc.2083

Subject(s) - chemistry , dephasing , spinning , spin echo , nuclear magnetic resonance , pulse sequence , dipole , spin (aerodynamics) , resonance (particle physics) , analytical chemistry (journal) , condensed matter physics , atomic physics , magnetic resonance imaging , physics , thermodynamics , chromatography , medicine , organic chemistry , polymer chemistry , radiology

Spin‐echo, double‐resonance (SEDOR) dipolar recoupling experiments are illustrated on an I = 1/2, S = 3/2 spin system for static and spinning samples. An 15 N 23 Na spin system is used to show that the simple pulse sequence is very effective in causing 15 N dipolar dephasing using either a 23 Na π/2 recoupling pulse or a long radio‐frequency (r.f.) recoupling pulse. Copyright © 2007 John Wiley & Sons, Ltd.

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