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Complete assignments of 1 H and 13 C NMR spectral data of nine surfactin isomers
Author(s) -
Tang JinShan,
Gao Hao,
Hong Kui,
Yu Yang,
Jiang MiaoMiao,
Lin HaiPeng,
Ye WenCai,
Yao XinSheng
Publication year - 2007
Publication title -
magnetic resonance in chemistry
Language(s) - English
Resource type - Journals
SCImago Journal Rank - 0.483
H-Index - 72
eISSN - 1097-458X
pISSN - 0749-1581
DOI - 10.1002/mrc.2048
Subject(s) - chemistry , heteronuclear single quantum coherence spectroscopy , surfactin , dept , carbon 13 nmr , two dimensional nuclear magnetic resonance spectroscopy , stereochemistry , strain (injury) , mass spectrometry , bacteria , bacillus subtilis , chromatography , medicine , biology , genetics
A new surfactin isomer (1) was isolated from a mangrove bacteria strain ‘ Bacillus sp’. Its structure was identified, and full assignments of 1 H and 13 C NMR spectral data were achieved for the first time by a combination of mass spectrometry and 1D and 2D NMR experiments including DEPT, 1 H 1 H COSY, HSQC, HMBC, TOCSY, ROESY, and HSQC‐TOCSY. The NMR spectral data of eight known analogs (2–9) are also reported. Copyright © 2007 John Wiley & Sons, Ltd.
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