Unambiguous NMR spectral assignments of salvinorin A | Zendy

Giner JoséLuis | Zendy; Kiemle David J. | Zendy; Kutrzeba Lukasz | Zendy; Zjawiony Jordan | Zendy

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Unambiguous NMR spectral assignments of salvinorin A

Author(s) -

Giner JoséLuis,

Kiemle David J.,

Kutrzeba Lukasz,

Zjawiony Jordan

Publication year - 2007

Publication title -

magnetic resonance in chemistry

Language(s) - English

Resource type - Journals

SCImago Journal Rank - 0.483

H-Index - 72

eISSN - 1097-458X

pISSN - 0749-1581

DOI - 10.1002/mrc.1972

Subject(s) - chemistry , heteronuclear single quantum coherence spectroscopy , hallucinogen , two dimensional nuclear magnetic resonance spectroscopy , carbon 13 nmr , stereochemistry , proton nmr , psychology , psychiatry

The complete assignments of the 1 H and 13 C NMR spectra of the hallucinogenic neoclerodane diterpenoid salvinorin A were determined in three different NMR solvents using HSQC, HMBC and COSY. Solvent systems are described that allow the resolution of all 1 H signals. Virtual coupling was observed for the protons at C‐2, C‐3 and C‐4 in the 600 MHz 1 H spectrum in CDCl 3 . The complete assignments of the 1 H and 13 C NMR spectra of salvinorin B are also reported. Copyright © 2007 John Wiley & Sons, Ltd.

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