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1 H and 13 C NMR studies of 2‐functionalized 5‐(methylsulfonyl)‐1‐phenyl‐1 H ‐indoles
Author(s) -
CruzLópez Olga,
Gallo Miguel A.,
Espinosa Antonio,
Campos Joaquín M.
Publication year - 2007
Publication title -
magnetic resonance in chemistry
Language(s) - English
Resource type - Journals
SCImago Journal Rank - 0.483
H-Index - 72
eISSN - 1097-458X
pISSN - 0749-1581
DOI - 10.1002/mrc.1935
Subject(s) - chemistry , dept , substituent , moiety , indole test , carbon 13 nmr , proton nmr , stereochemistry , medicinal chemistry
The 1 H and 13 C NMR resonances of thirty 2‐functionalized 5‐(methylsulfonyl)‐1‐phenyl‐1 H ‐indoles were assigned completely and unequivocally using the concerted application of one‐ and two‐dimensional experiments (DEPT, gs‐HMQC and gs‐HMBC). Finally, the influence of the 2‐substituent of 5‐(methylsufonyl)‐1‐phenyl‐1 H ‐indoles on the carbon atoms of the indole moiety was estimated. Copyright © 2006 John Wiley & Sons, Ltd.