Total assignments of  1 H and  13 C NMR spectra of isocatalpanol and a derivative of tecomaquinone | Zendy

Santos Allana Kellen L. | Zendy; Assunção Jõao Carlos | Zendy; Fonseca Aluisio M. | Zendy; Pessoa Otilia D. L. | Zendy; Monte Francisco Jose Q. | Zendy; Lemos Telma L. G. | Zendy; BrazFilho Raimundo | Zendy

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Total assignments of 1 H and 13 C NMR spectra of isocatalpanol and a derivative of tecomaquinone

Author(s) -

Santos Allana Kellen L.,

Assunção Jõao Carlos,

Fonseca Aluisio M.,

Pessoa Otilia D. L.,

Monte Francisco Jose Q.,

Lemos Telma L. G.,

BrazFilho Raimundo

Publication year - 2005

Publication title -

magnetic resonance in chemistry

Language(s) - English

Resource type - Journals

SCImago Journal Rank - 0.483

H-Index - 72

eISSN - 1097-458X

pISSN - 0749-1581

DOI - 10.1002/mrc.1582

Subject(s) - chemistry , derivative (finance) , mass spectrum , mass spectrometry , lippia , nmr spectra database , spectral line , electron ionization , nuclear magnetic resonance spectroscopy , analytical chemistry (journal) , ionization , stereochemistry , organic chemistry , ion , physics , chromatography , essential oil , financial economics , economics , astronomy

Isocatalpanol and tecomaquinone I were obtained from roots of Lippia sidoides , a medicinal plant from northeast Brazil. Reduction of tecomaquinone I with NaBH 4 yielded a new derivative. Structural elucidation was done on the basis of spectral data, mainly by high‐field NMR and electron ionization mass spectrometry. Copyright © 2005 John Wiley & Sons, Ltd.

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