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Complete 1 H and 13 C NMR spectral assignment of 17‐hydroxy epimeric sterols with planar A or A and B rings
Author(s) -
Ciuffreda P.,
Casati S.,
Manzocchi A.
Publication year - 2004
Publication title -
magnetic resonance in chemistry
Language(s) - English
Resource type - Journals
SCImago Journal Rank - 0.483
H-Index - 72
eISSN - 1097-458X
pISSN - 0749-1581
DOI - 10.1002/mrc.1342
Subject(s) - chemistry , epimer , dept , two dimensional nuclear magnetic resonance spectroscopy , stereochemistry , heteronuclear single quantum coherence spectroscopy , nuclear magnetic resonance spectroscopy
Complete 1 H and 13 C spectral assignments of 17β‐ and 17α‐hydroxy epimers of three biologically active sterols (boldenone, 3‐methoxyestradiol and 3‐methoxydihydroequilenin) were achieved making use of one‐ and two‐dimensional NMR techniques (1D‐HOHAHA, DEPT, COSY, NOESY, TOCSY, HSQC and COLOC). Copyright © 2004 John Wiley & Sons, Ltd.