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Assignment of 1 H and 13 C NMR data for diethyl 2‐ and 8‐quinolylmethylphosphonates and their palladium(II) dihalide complexes
Author(s) -
Marinić Željko,
Ćurić Manda,
VikićTopić Dražen,
TušekBožić Ljerka
Publication year - 2003
Publication title -
magnetic resonance in chemistry
Language(s) - English
Resource type - Journals
SCImago Journal Rank - 0.483
H-Index - 72
eISSN - 1097-458X
pISSN - 0749-1581
DOI - 10.1002/mrc.1286
Subject(s) - chemistry , heteronuclear molecule , palladium , carbon 13 nmr , stereochemistry , nuclear magnetic resonance spectroscopy , medicinal chemistry , organic chemistry , catalysis
1 H and 13 C NMR spectral data for diethyl 2‐ and 8‐quinolylmethylphosphonates (L) and their palladium(II) dihalide complexes, trans ‐[PdL 2 X 2 ] (L = 2‐dqmp, 8‐dqmp; X = Cl, Br), are presented. The NMR analysis was performed on the basis of one‐ and two‐dimensional homo‐ and heteronuclear experiments including 1 H, 13 C, APT, 1 H– 1 H COSY, 1 H– 13 C COSY, HMQC and HMBC techniques. Copyright © 2003 John Wiley & Sons, Ltd.