High resolution  13 C and  1 H NMR spectral analysis of 1‐azafluorene | Zendy

Fomichov A. A. | Zendy; Svoren V. A. | Zendy; Golovtsov N. I. | Zendy; Soldatenkov A. T. | Zendy; Prostakov N. S. | Zendy

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High resolution 13 C and 1 H NMR spectral analysis of 1‐azafluorene

Author(s) -

Fomichov A. A.,

Svoren V. A.,

Golovtsov N. I.,

Soldatenkov A. T.,

Prostakov N. S.

Publication year - 1982

Publication title -

organic magnetic resonance

Language(s) - English

Resource type - Journals

SCImago Journal Rank - 0.483

H-Index - 72

eISSN - 1097-458X

pISSN - 0030-4921

DOI - 10.1002/mrc.1270190107

Subject(s) - heteronuclear molecule , chemistry , coupling constant , resonance (particle physics) , spectral line , pyridine , analytical chemistry (journal) , nmr spectra database , resolution (logic) , nuclear magnetic resonance spectroscopy , physics , atomic physics , stereochemistry , medicinal chemistry , organic chemistry , particle physics , astronomy , artificial intelligence , computer science

An analysis of the 1 H and 13 C spectra of 1‐azafluorene has been carried out using computer calculations and homo‐ and heteronuclear double resonance techniques. The 4 J , 5 J and 6 J long‐range coupling constants of the 9‐CH 2 group protons with the protons of the pyridine and the phenylene rings have been observed and measured. The long‐range J (CH) values in the 1 H coupled 13 C spectrum have been assigned and measured on a first‐order basis.

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