Deuterium nuclear magnetic resonance spectroscopy. II —distribution of deuterium in some labelled nitrogen heterocyclic compounds | Zendy

AlRawi Jasim M. A. | Zendy; Behnam George Q. | Zendy; Taha Nihad I. | Zendy

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Deuterium nuclear magnetic resonance spectroscopy. II —distribution of deuterium in some labelled nitrogen heterocyclic compounds

Author(s) -

AlRawi Jasim M. A.,

Behnam George Q.,

Taha Nihad I.

Publication year - 1981

Publication title -

organic magnetic resonance

Language(s) - English

Resource type - Journals

SCImago Journal Rank - 0.483

H-Index - 72

eISSN - 1097-458X

pISSN - 0030-4921

DOI - 10.1002/mrc.1270170315

Subject(s) - deuterium , isoquinoline , quinoline , chemistry , nuclear magnetic resonance spectroscopy , labelling , pyridine , deuterium nmr , nitrogen , spectroscopy , radiochemistry , heavy water , platinum , nuclear magnetic resonance , organic chemistry , catalysis , nuclear physics , biochemistry , physics , quantum mechanics

Pyridine, methylpyridines, quinoline and isoquinoline have been labelled with deuterium using pre‐reduced platinum dioxide (PtO 2 ·2H 2 O) and heavy water. Their 2 H chemical shifts from monodeuteriated TMS have been assigned. The extent of the labelling has been determined directly by 2 H NMR spectroscopy.

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