17 O nuclear magnetic resonance studies of some amino acids at natural abundance | Zendy

Valentine B. | Zendy; Amour T. St | Zendy; Walter R. | Zendy; Fiat D. | Zendy

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17 O nuclear magnetic resonance studies of some amino acids at natural abundance

Author(s) -

Valentine B.,

Amour T. St,

Walter R.,

Fiat D.

Publication year - 1980

Publication title -

organic magnetic resonance

Language(s) - English

Resource type - Journals

SCImago Journal Rank - 0.483

H-Index - 72

eISSN - 1097-458X

pISSN - 0030-4921

DOI - 10.1002/mrc.1270130318

Subject(s) - abundance (ecology) , amino acid , nuclear magnetic resonance , natural abundance , resonance (particle physics) , chemistry , sensitivity (control systems) , solvent , chemical shift , analytical chemistry (journal) , physics , atomic physics , biology , environmental chemistry , chromatography , ecology , biochemistry , mass spectrometry , electronic engineering , engineering

17 O chemical shifts of four amino acids at natural abundance have been obtained. Sensitivity was enhanced by accumulating a large number of scans or employing high concentrations at elevated temperature. Routine memory overflow was avoided by using a combination of solvent suppression and phase alternating pulse sequences.

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