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A general purpose n.m.r. microcell system suitable for volatile, air sensitive and toxic samples
Author(s) -
AlRawi Jassim M. A.,
Bloxsidge James P.
Publication year - 1977
Publication title -
organic magnetic resonance
Language(s) - English
Resource type - Journals
SCImago Journal Rank - 0.483
H-Index - 72
eISSN - 1097-458X
pISSN - 0030-4921
DOI - 10.1002/mrc.1270100161
Subject(s) - microcell , tube (container) , chromatography , materials science , analytical chemistry (journal) , chemistry , composite material , engineering , telecommunications
A microcell system that is convenient to fill and which can be evacuated and/or filled with gas or vapour has been developed for handling tritiated n.m.r. samples and has subsequently proved to have a more general application. A 3 mm tube, after the removal of a 5 mm filling extension, is sleeved into a 5 mm n.m.r. tube or used directly in a reduced diameter probe.
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