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An instrumental modification for rapid‐scan deuterium magnetic resonance spectroscopy
Author(s) -
Bloxsidge James P.
Publication year - 1977
Publication title -
organic magnetic resonance
Language(s) - English
Resource type - Journals
SCImago Journal Rank - 0.483
H-Index - 72
eISSN - 1097-458X
pISSN - 0030-4921
DOI - 10.1002/mrc.1270091014
Subject(s) - deuterium , spectrometer , fourier transform , nuclear magnetic resonance , fourier transform spectroscopy , sensitivity (control systems) , spectroscopy , analytical chemistry (journal) , lock (firearm) , materials science , channel (broadcasting) , fourier transform infrared spectroscopy , chemistry , optics , atomic physics , physics , computer science , telecommunications , electronic engineering , engineering , chromatography , mechanical engineering , quantum mechanics
Abstract A modification of a Bruker WH‐90 spectrometer is reported, enabling acquisition of rapid‐scan (Fourier transform correlation) deuterium magnetic resonance spectra, using the D‐lock frequency source and a computer generated field sweep. This modification is not suited to high sensitivity or high precision studies, but does avoid the considerable expense or extensive rebuilding required for a 19 F lock channel and 2 H pulsed Fourier channel.