Peak suppression in Fourier transform n.m.r.: Application of the selective excitation technique to the problem of  13 C satellites in  31 P resonance | Zendy

Harris R. K. | Zendy; Newman R. H. | Zendy; Okruszek A. | Zendy

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Peak suppression in Fourier transform n.m.r.: Application of the selective excitation technique to the problem of 13 C satellites in 31 P resonance

Author(s) -

Harris R. K.,

Newman R. H.,

Okruszek A.

Publication year - 1977

Publication title -

organic magnetic resonance

Language(s) - English

Resource type - Journals

SCImago Journal Rank - 0.483

H-Index - 72

eISSN - 1097-458X

pISSN - 0030-4921

DOI - 10.1002/mrc.1270090113

Subject(s) - excitation , resonance (particle physics) , fourier transform , analytical chemistry (journal) , isotopomers , nuclear magnetic resonance , physics , range (aeronautics) , chemistry , atomic physics , materials science , spectral line , chromatography , quantum mechanics , composite material , astronomy

Selective pulsed excitation was used in a technique to suppress the resonance due to a per‐ 12 C‐isotopomer so as to overcome dynamic range problems when observing ‘ 13 C satellite’ lines. The technique was used to obtain nuclear spin parameters from the 13 C satellites in 31 P resonance for the racemic isomer of P , P ′‐dimethyl‐ P , P ′‐diphenyldiphosphine disulphide, [MePhP(:S)] 2 .

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