Complete assignment of the  13 C n.m.r. spectrum of mutarotated  D ‐ribose by integration and specific deuteration | Zendy

Breitmaier E. | Zendy; Hollstein U. | Zendy

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Complete assignment of the 13 C n.m.r. spectrum of mutarotated D ‐ribose by integration and specific deuteration

Author(s) -

Breitmaier E.,

Hollstein U.

Publication year - 1976

Publication title -

organic magnetic resonance

Language(s) - English

Resource type - Journals

SCImago Journal Rank - 0.483

H-Index - 72

eISSN - 1097-458X

pISSN - 0030-4921

DOI - 10.1002/mrc.1270081108

Subject(s) - ribose , furanose , spectrum (functional analysis) , pyranose , chemistry , stereochemistry , crystallography , physics , biochemistry , organic chemistry , quantum mechanics , ring (chemistry) , enzyme

The 13 C n.m.r. spectrum of mutarotated D ‐ribose is completely assigned by using 2‐ and 3‐deuterio‐ D ‐ribose as reference compounds. The signal intensities of the largely relaxed 13 C n.m.r. spectrum are evaluated, and the equilibrium mixture of mutarotated D ‐ribose is found to consist of 6·1% α‐furanose, 11·6% β‐furanose, 20·3% α‐pyranose and 62% β‐pyranose.

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