High resolution  13 C spectroscopy by Fourier transform NMR. Thiete sulfone | Zendy

Levy George C. | Zendy; Dittmer Donald C. | Zendy

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High resolution 13 C spectroscopy by Fourier transform NMR. Thiete sulfone

Author(s) -

Levy George C.,

Dittmer Donald C.

Publication year - 1972

Publication title -

organic magnetic resonance

Language(s) - English

Resource type - Journals

SCImago Journal Rank - 0.483

H-Index - 72

eISSN - 1097-458X

pISSN - 0030-4921

DOI - 10.1002/mrc.1270040112

Subject(s) - decoupling (probability) , sulfone , fourier transform , resolution (logic) , fourier transform spectroscopy , spectroscopy , high resolution , nuclear magnetic resonance , nuclear magnetic resonance spectroscopy , chemistry , analytical chemistry (journal) , materials science , physics , computer science , organic chemistry , quantum mechanics , control engineering , engineering , remote sensing , artificial intelligence , geology

The high resolution 13 C NMR spectrum of thiete sulfone (obtained without wide‐band 1 H decoupling) indicates that ring strain and re‐hybridization in this small ring compound are significant. Pulsed‐Fourier operation allows rapid determination of spectral parameters. Experimental acquisition time by pulsed NMR without 1 H decoupling is comparable to the experimental time required for swept 13 C NMR with complete 1 H decoupling.

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