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Tritium nuclear magnetic resonance spectroscopy—I: Technique, internal referencing and some preliminary results
Author(s) -
Bloxsidge J.,
Elvidge J. A.,
Jones J. R.,
Evans E. A.
Publication year - 1971
Publication title -
organic magnetic resonance
Language(s) - English
Resource type - Journals
SCImago Journal Rank - 0.483
H-Index - 72
eISSN - 1097-458X
pISSN - 0030-4921
DOI - 10.1002/mrc.1270030112
Subject(s) - radiolysis , chemistry , uridine , radiochemistry , natural abundance , nuclear magnetic resonance , spectroscopy , isotope , analytical chemistry (journal) , mass spectrometry , nuclear physics , physics , chromatography , aqueous solution , biochemistry , rna , quantum mechanics , gene
Routine measurement of triton magnetic resonance spectra is described for the first time, using a micro‐bulb sample tube assembly to obviate radiological hazards. Levels of isotope abundance and chemical concentration, the problem of self‐radiolysis and the general usefulness of the technique are discussed. Results are given for a selection of compounds including glucose, amino‐acids, thymidine and uridine. The self‐radiolysis of the last is followed.