Rapid method for combined X—{ 1 H} NOE and  T  1  measurement using heteronuclear polarization transfer | Zendy

Kövér Katalin E. | Zendy; Forgó Péter | Zendy; Batta Gyula | Zendy

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Rapid method for combined X—{ 1 H} NOE and T 1 measurement using heteronuclear polarization transfer

Author(s) -

Kövér Katalin E.,

Forgó Péter,

Batta Gyula

Publication year - 1995

Publication title -

magnetic resonance in chemistry

Language(s) - English

Resource type - Journals

SCImago Journal Rank - 0.483

H-Index - 72

eISSN - 1097-458X

pISSN - 0749-1581

DOI - 10.1002/mrc.1260331105

Subject(s) - heteronuclear molecule , chemistry , polarization (electrochemistry) , analytical chemistry (journal) , nuclear magnetic resonance , nuclear magnetic resonance spectroscopy , chromatography , stereochemistry , physics

A polarization transfer enhanced inversion‐recovery experiment is proposed for the combined measurement of heteronuclear T 1 and NOE of low‐γ nuclei. This method offers significant time savings compared with conventional relaxation measurements. The reliability and accuracy of the combined T 1 , and NOE determination and its dependence on the experimental set‐up is also demonstrated. The proposed approach may be preferred for multiple field/multiple temperature model‐free analysis of molecular dynamics.

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