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Analysis of the 13 C and 1 H spectra of mixtures of benzylidene derivatives
Author(s) -
Bradley J. C.,
Williams A. J.
Publication year - 1994
Publication title -
magnetic resonance in chemistry
Language(s) - English
Resource type - Journals
SCImago Journal Rank - 0.483
H-Index - 72
eISSN - 1097-458X
pISSN - 0749-1581
DOI - 10.1002/mrc.1260320812
Subject(s) - chemistry , spectral line , nmr spectra database , ring (chemistry) , carbon 13 nmr , stereochemistry , organic chemistry , physics , astronomy
The 1 H and 13 C NMR spectra of methyl ( E )‐2,3,‐diphenylprop‐2‐enoate and methyl ( E )‐2‐(2‐phenylethenyl) benzoate resulting from the electrocyclic ring opening of benzocyclobutenone starting materials have been assigned. A combination of direct detection 2D NMR techniques, COSY, HETCOR and FLOCK, provided the assignments of the 1 H and 13 C resonances.
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