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Structural analysis of oligosaccharide chains of glycolipids by two‐dimensional NMR
Author(s) -
Inagaki Fuyuhiko
Publication year - 1992
Publication title -
magnetic resonance in chemistry
Language(s) - English
Resource type - Journals
SCImago Journal Rank - 0.483
H-Index - 72
eISSN - 1097-458X
pISSN - 0749-1581
DOI - 10.1002/mrc.1260301321
Subject(s) - chemistry , oligosaccharide , glycolipid , monosaccharide , homonuclear molecule , two dimensional nuclear magnetic resonance spectroscopy , nuclear magnetic resonance spectroscopy , stereochemistry , molecule , organic chemistry , biochemistry
Coherence transfer methods, such as multiple‐relayed COSY and homonuclear Hartman–Hahn spectroscopy, were applied to extract subspectra of constituent monosaccharides, which allowed complete assignments of the proton resonances of oligosaccharide chains of glycolipids. The chemical structure of oligosaccharide chains of glycolipids could be determined by the combination of coherence transfer methods and NOESY experiments.