Comparison of different 2D NMR techniques for  13 C,  31 P correlation | Zendy

Bast Peter | Zendy; Berger Stefan | Zendy; Günther Harald | Zendy

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Comparison of different 2D NMR techniques for 13 C, 31 P correlation

Author(s) -

Bast Peter,

Berger Stefan,

Günther Harald

Publication year - 1992

Publication title -

magnetic resonance in chemistry

Language(s) - English

Resource type - Journals

SCImago Journal Rank - 0.483

H-Index - 72

eISSN - 1097-458X

pISSN - 0749-1581

DOI - 10.1002/mrc.1260300704

Subject(s) - chemistry , nicotinamide adenine dinucleotide , correlation , analytical chemistry (journal) , two dimensional nuclear magnetic resonance spectroscopy , nuclear magnetic resonance spectroscopy , polarization (electrochemistry) , nuclear magnetic resonance , nad+ kinase , chromatography , stereochemistry , physics , enzyme , organic chemistry , geometry , mathematics

Three different experimental techniques are compared to find the most efficient protocol for 2D 13 C, 31 P correlation spectroscopy. It is shown that the best signal‐to‐noise ratio is given by the polarization transfer experiment for 31 P detection and by the HMQC experiment for 13 C detection. Applications of these techniques for 13 C, 31 P correlation of β‐nicotinamide adenine dinucleotide (NAD + ) and a mixture of three different mononucleotides are described.

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