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Applications of two‐dimensional NMR in spectral assignments of the cytotoxic triterpene saponaceolide B
Author(s) -
Geraci Corrada,
Piattelli Mario,
Tringali Corrado
Publication year - 1991
Publication title -
magnetic resonance in chemistry
Language(s) - English
Resource type - Journals
SCImago Journal Rank - 0.483
H-Index - 72
eISSN - 1097-458X
pISSN - 0749-1581
DOI - 10.1002/mrc.1260290611
Subject(s) - chemistry , triterpene , two dimensional nuclear magnetic resonance spectroscopy , stereochemistry , cytotoxic t cell , nuclear magnetic resonance spectroscopy , nmr spectra database , spectral line , in vitro , biochemistry , medicine , alternative medicine , pathology , physics , astronomy
COSY, one‐bond and long‐range HETCOR NMR spectra were used in combination for the complete 1 H and 13 C assignments of the cytotoxic triterpene saponaceolide B. Stereochemical assignments were based on a NOESY spectrum.
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