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Complete 1 H and 13 C NMR spectral assignment of some polynitropolycyclic cage molecules by 2D NMR spectroscopy
Author(s) -
Axenrod T.,
Liang B.,
Dave P. R.
Publication year - 1991
Publication title -
magnetic resonance in chemistry
Language(s) - English
Resource type - Journals
SCImago Journal Rank - 0.483
H-Index - 72
eISSN - 1097-458X
pISSN - 0749-1581
DOI - 10.1002/mrc.1260290104
Subject(s) - chemistry , molecule , nmr spectra database , spectral line , nuclear magnetic resonance spectroscopy , two dimensional nuclear magnetic resonance spectroscopy , carbon 13 nmr satellite , crystallography , transverse relaxation optimized spectroscopy , spectroscopy , carbon 13 nmr , fluorine 19 nmr , stereochemistry , organic chemistry , physics , quantum mechanics , astronomy
The 1 H and 13 C NMR spectra of several saturated polynitropolycyclic molecules were unambiguously assigned using aromatic solvent‐induced shifts, NOE difference spectra, 1 H– 1 H COSY spectra and 2D 13 C– 1 H shift correlated spectra, optimized either for one‐bond or long‐range 13 C– 1 H couplings.