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1 H and 13 C NMR spectra of pseudomorphine and dimethylpseudomorphine
Author(s) -
Graden D. W.,
Caldwell G. W.,
Villani F. J.,
Maryanoff C. A.,
Grant A.
Publication year - 1990
Publication title -
magnetic resonance in chemistry
Language(s) - English
Resource type - Journals
SCImago Journal Rank - 0.483
H-Index - 72
eISSN - 1097-458X
pISSN - 0749-1581
DOI - 10.1002/mrc.1260281204
Subject(s) - chemistry , dept , two dimensional nuclear magnetic resonance spectroscopy , nmr spectra database , spectral line , carbon 13 nmr , pulse sequence , proton , nuclear magnetic resonance spectroscopy , stereochemistry , analytical chemistry (journal) , nuclear magnetic resonance , organic chemistry , physics , nuclear physics , astronomy
The 1 H and 13 C NMR spectra of 7,7′,8,8′‐tetradehydro‐4,5:4′,5′‐diepoxy‐17,17′‐dimethyl‐[2,2′‐bimorphinan]‐3,3′,6,6′‐tetrol; [2,2′‐bimorphine] (pseudomorphine) and 7,7′,8,8′‐tetradehydro‐4,5:4′,5′‐diepoxy‐17,17′‐dimethyl‐[2,2′‐bimorphinan]‐3,3′‐dimethoxy‐6,6′‐diol; 2,2′‐bimorphine (dimethylpseudomorphine) were measured and assigned using DEPT, COSY, HETCOR, NOESY, NOE difference techniques and selective proton decoupled carbon NMR experiments.