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Partial editing in heteronuclear J ‐resolved solid‐state NMR spectroscopy
Author(s) -
Tekely P.,
Brondeau J.,
Retournard A.,
Canet D.
Publication year - 1989
Publication title -
magnetic resonance in chemistry
Language(s) - English
Resource type - Journals
SCImago Journal Rank - 0.483
H-Index - 72
eISSN - 1097-458X
pISSN - 0749-1581
DOI - 10.1002/mrc.1260270718
Subject(s) - heteronuclear molecule , chemistry , decoupling (probability) , nuclear magnetic resonance spectroscopy , solid state , solid state nuclear magnetic resonance , pulse sequence , spectroscopy , spectral line , sequence (biology) , analytical chemistry (journal) , nuclear magnetic resonance , crystallography , stereochemistry , chromatography , physics , biochemistry , quantum mechanics , control engineering , astronomy , engineering
A solid‐state analogue of the double echo sequence and gated decoupling used previously for the determination of carbon multiplicities in liquids is described; it was applied to the simplification and assignment of 13 C CP‐MAS spectra in solids. This procedure permits partially edited 13 C CP‐MAS subspectra to be obtained directly by means of distinct experiments performed under an identical length of the evolution period.