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Structure elucidation of an unexpected acylation product of dithranol: An application of improved heteronuclear two‐dimensional NOE spectroscopy
Author(s) -
Bigler P.,
Rychener M.,
Séquin U.
Publication year - 1988
Publication title -
magnetic resonance in chemistry
Language(s) - English
Resource type - Journals
SCImago Journal Rank - 0.483
H-Index - 72
eISSN - 1097-458X
pISSN - 0749-1581
DOI - 10.1002/mrc.1260260706
Subject(s) - heteronuclear molecule , chemistry , dithranol , acylation , pulse sequence , nuclear magnetic resonance spectroscopy , product (mathematics) , stereochemistry , organic chemistry , nuclear magnetic resonance , medicine , physics , geometry , mathematics , dermatology , psoriasis , catalysis
Heteronuclear NOEs have proved to be a valuable tool for the structure elucidation of an unexpected acylation product of dithranol. The application of a modified 2D HOESY pulse sequence with improved sensitivity is demonstrated.