Two‐dimensional  1 H and  13 C‐NMR spectra of 5‐(2‐dimethylaminoethoxy)‐7‐oxo‐7 H ‐benzo[ c ]fluorene, its precursor and metabolite | Zendy

Lyčka Antonin | Zendy; Jirman Josef | Zendy; Nobilis Milan | Zendy; Kvasničková Eva | Zendy; Hais Ivo M. | Zendy

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Two‐dimensional 1 H and 13 C‐NMR spectra of 5‐(2‐dimethylaminoethoxy)‐7‐oxo‐7 H ‐benzo[ c ]fluorene, its precursor and metabolite

Author(s) -

Lyčka Antonin,

Jirman Josef,

Nobilis Milan,

Kvasničková Eva,

Hais Ivo M.

Publication year - 1987

Publication title -

magnetic resonance in chemistry

Language(s) - English

Resource type - Journals

SCImago Journal Rank - 0.483

H-Index - 72

eISSN - 1097-458X

pISSN - 0749-1581

DOI - 10.1002/mrc.1260251207

Subject(s) - chemistry , fluorene , spectral line , nmr spectra database , metabolite , nuclear magnetic resonance spectroscopy , stereochemistry , organic chemistry , physics , biochemistry , polymer , astronomy

The 1 H and 13 C chemical shifts in 5‐(2‐dimethylaminoethoxy)‐7‐oxo‐7 H ‐benzo[ c ]fluorene (1) and 5‐hydroxy‐7‐oxo‐7 H ‐benzo[ c ]fluorene (2) were assigned using H,H‐COSY, H,C‐COSY and selective INEPT spectra. It was found that the main phenolic metabolite of 1 and its hydrochloride corresponds to 9‐hydroxy‐5‐(2‐dimethylaminoethoxy)‐7‐oxo‐7 H ‐benzo[ c ]fluorene (3).

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