Correlated  1 H 13 C NMR spectroscopy of peracetylated glycosphingolipids at 500 MHz | Zendy

Dabrowski Janusz | Zendy; Dabrowski Ursula | Zendy; Hanfland Peter | Zendy; Kordowicz Maria | Zendy; Hull William E. | Zendy

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Correlated 1 H 13 C NMR spectroscopy of peracetylated glycosphingolipids at 500 MHz

Author(s) -

Dabrowski Janusz,

Dabrowski Ursula,

Hanfland Peter,

Kordowicz Maria,

Hull William E.

Publication year - 1986

Publication title -

magnetic resonance in chemistry

Language(s) - English

Resource type - Journals

SCImago Journal Rank - 0.483

H-Index - 72

eISSN - 1097-458X

pISSN - 0749-1581

DOI - 10.1002/mrc.1260240820

Subject(s) - chemistry , ceramide , spectroscopy , nuclear magnetic resonance spectroscopy , membrane , dept , stereochemistry , biochemistry , apoptosis , physics , quantum mechanics

The assignments of the sugar and ceramide 13 C and 1 H signals of peracetylated ceramide penta‐ and deca‐saccharide from rabbit erythrocyte membranes, viz. Galα(1→3)Galβ(→4)GlcNAcβ(1→3)Galβ(1→4)Glcβ(1→1) Cer (Cer=ceramide) and Galα(1→3)Galβ(1→4)GlcNAcα(1→3[)Galβ(1→4)GlcNAcβ(1→6)]GalNAcβ(1→4)GlcNAcβ(1→3)Galβ(1→4)Glcβ(1→1)Cer, were obtained by the combined use of homo‐ and hetero‐nuclear shift‐correlated 2D and DEPT spectra. A few ambiguities resulting from exact coincidence of 1 H resonances were resolved by relying on reference data for similar environments.

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