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Application of two‐dimensional correlated NMR techniques to the structure elucidation of 1‐methoxy‐ endo ‐tetracyclo[6.3.0.0 2,11 .0 3,7 ]‐ undec‐9‐ene
Author(s) -
Kruk C.,
Jans A. W. H.,
Cornelisse J.,
Lugtenburg J.
Publication year - 1985
Publication title -
magnetic resonance in chemistry
Language(s) - English
Resource type - Journals
SCImago Journal Rank - 0.483
H-Index - 72
eISSN - 1097-458X
pISSN - 0749-1581
DOI - 10.1002/mrc.1260230906
Subject(s) - chemistry , ene reaction , nuclear magnetic resonance spectroscopy , proton , chemical shift , spectroscopy , stereochemistry , two dimensional nuclear magnetic resonance spectroscopy , proton nmr , carbon 13 nmr , physics , quantum mechanics
By means of 500 MHz 1 H two‐dimensional correlated NMR spectroscopy and the 62.89 MHz 13 C two‐dimensional Inadequate technique, all proton and carbon chemical shifts of 1‐methoxy‐ endo ‐tetracy‐clo[6.3.0.0 2,11 .0 3,7 ]undec‐9‐eene can be assigned in an unambiguous way.