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Concerted use of two‐dimensional NMR techniques in the ab initio assignment of complex spectra: Complete proton and carbon‐13 assignment of oligomycin A
Author(s) -
Morris Gareth A.,
Richards Michelle S.
Publication year - 1985
Publication title -
magnetic resonance in chemistry
Language(s) - English
Resource type - Journals
SCImago Journal Rank - 0.483
H-Index - 72
eISSN - 1097-458X
pISSN - 0749-1581
DOI - 10.1002/mrc.1260230815
Subject(s) - homonuclear molecule , heteronuclear molecule , chemistry , spectral line , nmr spectra database , carbon 13 nmr , ab initio , proton , two dimensional nuclear magnetic resonance spectroscopy , nuclear magnetic resonance , computational chemistry , nuclear magnetic resonance spectroscopy , stereochemistry , molecule , organic chemistry , physics , nuclear physics , astronomy
The identification and complete 13 C and 1 H assignment of a sample of oligomycin A is described. 13 C multiplicities were determined by the INEPT method; assignments were made by comparison of heteronuclear 13 C‐ 1 H chemical shift correlation, homonuclear COSY and homonuclear relayed coherence transfer two‐dimensional NMR spectra.