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Analysis of the NMR spectra of trimethylsilyl‐substituted sugars by two‐dimensional heteronuclear 29 Si– 1 H shift correlation spectroscopy
Author(s) -
Liepinsh E.,
Sekacis I.,
Lukevics E.
Publication year - 1985
Publication title -
magnetic resonance in chemistry
Language(s) - English
Resource type - Journals
SCImago Journal Rank - 0.483
H-Index - 72
eISSN - 1097-458X
pISSN - 0749-1581
DOI - 10.1002/mrc.1260230105
Subject(s) - chemistry , trimethylsilyl , heteronuclear molecule , nuclear magnetic resonance spectroscopy , spectral line , nmr spectra database , spectroscopy , analytical chemistry (journal) , computational chemistry , stereochemistry , organic chemistry , physics , quantum mechanics , astronomy
Two‐dimensional NMR experiments on 29 Si‐ 1 H shift correlations in trimethylsilyl‐substituted sugars are described. This technique allows the unambiguous assignment of 29 Si and 1 H signals of all trimethylsilyl groups.