Isolation and characterization of a Tie2 kinase inhibitory sulfated triterpenoid from a green alga of the  Tuemoya  genus: complete assignment of the  1 H and  13 C spectra of a sulfated triterpenoid Tie2 kinase inhibitor | Zendy

Clement Jason A. | Zendy; Zhou BingNan | Zendy; Johnson Randall K. | Zendy; Kingston David G. I. | Zendy

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Isolation and characterization of a Tie2 kinase inhibitory sulfated triterpenoid from a green alga of the Tuemoya genus: complete assignment of the 1 H and 13 C spectra of a sulfated triterpenoid Tie2 kinase inhibitor

Author(s) -

Clement Jason A.,

Zhou BingNan,

Johnson Randall K.,

Kingston David G. I.

Publication year - 2003

Publication title -

magnetic resonance in chemistry

Language(s) - English

Resource type - Journals

SCImago Journal Rank - 0.483

H-Index - 72

eISSN - 1097-458X

pISSN - 0749-1581

DOI - 10.1002/mrc.1228

Subject(s) - chemistry , triterpenoid , sulfation , stereochemistry , fractionation , enzyme , two dimensional nuclear magnetic resonance spectroscopy , biochemistry , chromatography

Bioassay‐guided fractionation of an extract of a Tuemoya sp., using an assay for inhibitors of the enzyme Tie2 kinase, afforded a mixture of the sulfated cycloartanol triterpenoids 1 and 2. We report the full 1 H and 13 C NMR spectral assignments for 1 and the 13 C NMR spectral assignments for 2. Copyright © 2003 John Wiley & Sons, Ltd.

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