Synthesis and spectral study of a novel distamycin conjugate | Zendy

Pineda de las Infantas M. J. | Zendy; Campos J. | Zendy; Baraldi P. G. | Zendy; Romagnoli R. | Zendy; Gallo M. A. | Zendy; Espinosa A. | Zendy

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Synthesis and spectral study of a novel distamycin conjugate

Author(s) -

Pineda de las Infantas M. J.,

Campos J.,

Baraldi P. G.,

Romagnoli R.,

Gallo M. A.,

Espinosa A.

Publication year - 2003

Publication title -

magnetic resonance in chemistry

Language(s) - English

Resource type - Journals

SCImago Journal Rank - 0.483

H-Index - 72

eISSN - 1097-458X

pISSN - 0749-1581

DOI - 10.1002/mrc.1192

Subject(s) - chemistry , conjugate , pyrrole , dept , nuclear overhauser effect , stereochemistry , hydrochloride , proton nmr , carbon 13 nmr , nuclear magnetic resonance spectroscopy , organic chemistry , mathematical analysis , mathematics

The 1 H and 13 C NMR resonances for a novel distamycin conjugate, 3‐[1‐methyl‐4‐[1‐methyl‐4‐[1‐methyl‐4‐[N 1 ‐[5‐methyl‐2,4(1 H ,3 H )pyrimidinedione]acetylamino]pyrrole‐2‐carboxamido]pyrrole‐2‐carboxamido]pyrrole‐2‐carboxamido]propionamidine hydrochloride ( 1 ), were assigned, using the concerted application of one‐ and two‐dimensional NMR techniques including nuclear Overhauser effect difference, DEPT, HMQC and HMBC experiments. Copyright © 2003 John Wiley & Sons, Ltd.

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