Indirect detection of  31 P,X connectivities with proton sensitivity: application of two‐dimensional  31 P‐relayed  1 H,X correlation spectroscopy | Zendy

Gudat Dietrich | Zendy

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Indirect detection of 31 P,X connectivities with proton sensitivity: application of two‐dimensional 31 P‐relayed 1 H,X correlation spectroscopy

Author(s) -

Gudat Dietrich

Publication year - 2003

Publication title -

magnetic resonance in chemistry

Language(s) - English

Resource type - Journals

SCImago Journal Rank - 0.483

H-Index - 72

eISSN - 1097-458X

pISSN - 0749-1581

DOI - 10.1002/mrc.1172

Subject(s) - heteronuclear molecule , chemistry , spectroscopy , proton , analytical chemistry (journal) , nuclear magnetic resonance spectroscopy , crystallography , stereochemistry , physics , nuclear physics , chromatography , quantum mechanics

Experiments for 1 H‐detected heteronuclear 1 H,X correlation spectroscopy with 31 P‐relayed coherence transfer are described which allow the indirect detection of δX and n J (X,P) even in the absence of a direct J (X,H) coupling. The use of these techniques for the assignments of 13 C, 15 N, and 183 W NMR data of organophosphorus compounds is demonstrated. Copyright © 2003 John Wiley & Sons, Ltd.

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