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Structural determination and complete NMR spectral assignments of a new bufadienolide glycoside
Author(s) -
Ye Min,
Han Jian,
Guo Hongzhu,
Guo Dean
Publication year - 2002
Publication title -
magnetic resonance in chemistry
Language(s) - English
Resource type - Journals
SCImago Journal Rank - 0.483
H-Index - 72
eISSN - 1097-458X
pISSN - 0749-1581
DOI - 10.1002/mrc.1105
Subject(s) - chemistry , dept , heteronuclear single quantum coherence spectroscopy , glycoside , two dimensional nuclear magnetic resonance spectroscopy , stereochemistry , carbon 13 nmr , glucoside , medicine , alternative medicine , pathology
The structure of a new bufadienolide glycoside, cinobufagin 3‐ O ‐β‐ D ‐glucoside, was determined by extensive 1D and 2D NMR techniques ( 1 H, 13 C, DEPT, COSY, HSQC, g‐HMBC and NOESY). The complete assignments of the 13 C and 1 H spectral data were also carried out. Copyright © 2002 John Wiley & Sons, Ltd.
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