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1 H, 13 C, and 15 N NMR analysis of Tröger's base and of some of its [ 15 N 1 ] labelled precursors
Author(s) -
Salort Francisca,
Pardo Carmen,
Elguero José
Publication year - 2002
Publication title -
magnetic resonance in chemistry
Language(s) - English
Resource type - Journals
SCImago Journal Rank - 0.483
H-Index - 72
eISSN - 1097-458X
pISSN - 0749-1581
DOI - 10.1002/mrc.1091
Subject(s) - chemistry , chemical shift , coupling constant , carbon 13 nmr , base (topology) , spectral line , nitrogen , nmr spectra database , stereochemistry , organic chemistry , mathematical analysis , physics , mathematics , particle physics , astronomy
One‐ and two‐dimensional NMR spectra of Tröger's base, (±)‐2,8‐dimethyl‐6 H ,12 H ‐5,11‐methanodibenzo[ b,f ][1,5]diazocine labelled on one of the nitrogen atoms, have been used to determine the chemical shifts, coupling constants, and Δ 13 C( 15 N) isotope shifts. Copyright © 2002 John Wiley & Sons, Ltd.