Total assignment of  1 H and  13 C NMR spectra of three triterpene saponins from roots of  Silene vulgaris  (Moench) Garcke | Zendy

BouguetBonnet Sabine | Zendy; Rochd Mohamed | Zendy; Mutzenhardt Pierre | Zendy; Henry Max | Zendy

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Total assignment of 1 H and 13 C NMR spectra of three triterpene saponins from roots of Silene vulgaris (Moench) Garcke

Author(s) -

BouguetBonnet Sabine,

Rochd Mohamed,

Mutzenhardt Pierre,

Henry Max

Publication year - 2002

Publication title -

magnetic resonance in chemistry

Language(s) - English

Resource type - Journals

SCImago Journal Rank - 0.483

H-Index - 72

eISSN - 1097-458X

pISSN - 0749-1581

DOI - 10.1002/mrc.1069

Subject(s) - chemistry , triterpene , heteronuclear single quantum coherence spectroscopy , two dimensional nuclear magnetic resonance spectroscopy , glycoside , carbon 13 nmr , stereochemistry , nmr spectra database , caryophyllaceae , spectral line , botany , medicine , physics , alternative medicine , pathology , astronomy , biology

The assignments of 1 H and 13 C NMR spectra for three new triterpene saponins from Silene vulgaris (gypsogenin 3‐ O ‐glucuronide, quillaic acid 3‐ O ‐glucuronide, and gypsogenin 3‐ O ‐glycoside) are reported. In addition to 1D NMR methods, 2D NMR techniques (COSY, HSQC, HMBC, and HSQC‐TOCSY) were used for the assignments. Copyright © 2002 John Wiley & Sons, Ltd.

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