Preparation of Nylon‐6 Particles in Ionic Liquids | Zendy

Minami Hideto | Zendy; Tarutani Yasunori | Zendy; Yoshida Kazuhiro | Zendy; Okubo Masayoshi | Zendy

AI Assistant Blog Pricing

Home ZAIA Blog

Premium

Preparation of Nylon‐6 Particles in Ionic Liquids

Author(s) -

Minami Hideto,

Tarutani Yasunori,

Yoshida Kazuhiro,

Okubo Masayoshi

Publication year - 2010

Publication title -

macromolecular symposia

Language(s) - English

Resource type - Journals

SCImago Journal Rank - 0.257

H-Index - 76

eISSN - 1521-3900

pISSN - 1022-1360

DOI - 10.1002/masy.201050207

Subject(s) - ionic liquid , caprolactam , polymer chemistry , tetrafluoroborate , thermal stability , amide , materials science , polymerization , polymer , hydrolysis , nylon 6 , chemical engineering , chemistry , organic chemistry , composite material , engineering , catalysis

Summary: Utilizing the thermal stability of ionic liquid, micrometer‐sized Nylon‐6 particles were successfully prepared by hydrolytic polymerization of ε ‐caprolactam at high temperature with polyvinyl pyrrolidone as stabilizer in ionic liquids, 1‐butyl‐3‐methyl imidazolium tetrafluoroborate, [Bmim][BF 4 ] and N,N‐diethyl‐N‐methyl‐N‐(2‐methoxyethyl)ammonium bis(trifluoro‐methanesulfonyl)amide, [DEME][TFSA]. The obtained particles had a unique shape because Nylon‐6 is a crystalline polymer. Viscosity‐average molecular weights of Nylon‐6 prepared in [Bmim][BF 4 ] and [DEME][TFSA] at 180 °C for 48 h were 4200 and 2200, respectively.

This content is not available in your region!

Continue researching here.

Having issues? You can contact us here

Accelerating Research