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Minimization of carryover for high‐throughput liquid chromatography with tandem mass spectrometry analysis of 14 mycotoxins in corn grits
Author(s) -
Tamura Masayoshi,
Matsumoto Keiko,
Watanabe Jun,
Iida Junko,
Nagatomi Yasushi,
Mochizuki Naoki
Publication year - 2014
Publication title -
journal of separation science
Language(s) - English
Resource type - Journals
SCImago Journal Rank - 0.72
H-Index - 102
eISSN - 1615-9314
pISSN - 1615-9306
DOI - 10.1002/jssc.201470111
Subject(s) - mycotoxin , fumonisin , fumonisin b1 , chromatography , chemistry , contamination , mass spectrometry , tandem mass spectrometry , adsorption , tandem , environmental chemistry , food science , materials science , biology , organic chemistry , ecology , composite material
(J. Sep. Sci. 2014, 37 (13), 1552–1560) DOI: 10.1002/jssc.201400099 Corn is a major crop, but there is risk of contamination of mycotoxins. Because fumonisin, one of the mycotoxins, adsorb on the metal in the analyzer, there is a problem in analytical accuracy. Therefore, to suppress the adsorption of fumonisin, a method for the simultaneous analysis of 14 mycotoxins was developed. It could be shown that this newly developed method is highly sensitive and with high accuracy.