Separation, interconversion, and insecticidal activity of the  cis‐  and  trans ‐isomers of novel hydrazone derivatives | Zendy

Wu Jian | Zendy; Huang Chaoqun | Zendy; Wang Jian | Zendy; Hu Deyu | Zendy; Jin Linhong | Zendy; Yang Song | Zendy; Song Baoan | Zendy

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Separation, interconversion, and insecticidal activity of the cis‐ and trans ‐isomers of novel hydrazone derivatives

Author(s) -

Wu Jian,

Huang Chaoqun,

Wang Jian,

Hu Deyu,

Jin Linhong,

Yang Song,

Song Baoan

Publication year - 2013

Publication title -

journal of separation science

Language(s) - English

Resource type - Journals

SCImago Journal Rank - 0.72

H-Index - 102

eISSN - 1615-9314

pISSN - 1615-9306

DOI - 10.1002/jssc.201200693

Subject(s) - hydrazone , chemistry , cis–trans isomerism , isomerization , structural isomer , high performance liquid chromatography , medicinal chemistry , stereochemistry , chromatography , organic chemistry , catalysis

A series of cis ‐ and trans ‐isomers of hydrazone derivatives were separated and analyzed through HPLC with diode‐array detection and HPLC ‐ MS / MS using ESI and ion trap MS . Two single crystals ( A ‐5‐1 and C ‐2‐1) of the trans ‐isomers were obtained and determined using X ‐ray crystallography data, and the cis ‐ to trans ‐isomerization under different conditions was discussed. Both of the cis ‐ and trans ‐isomers of A ‐4 and A ‐5 exhibited good insecticidal activities against P lutella xylostella .

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