Near‐infrared fourier transform Raman microspectroscopy at high external pressures | Zendy

Barnett Steven M. | Zendy; Markwell Ross D. | Zendy; Brienne Stéphane H. R. | Zendy; Butler Ian S. | Zendy; Gilson Denis F. R. | Zendy; Kawai Nancy T. | Zendy; Vlček Antonín | Zendy

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Near‐infrared fourier transform Raman microspectroscopy at high external pressures

Author(s) -

Barnett Steven M.,

Markwell Ross D.,

Brienne Stéphane H. R.,

Butler Ian S.,

Gilson Denis F. R.,

Kawai Nancy T.,

Vlček Antonín

Publication year - 1993

Publication title -

journal of raman spectroscopy

Language(s) - English

Resource type - Journals

SCImago Journal Rank - 0.748

H-Index - 110

eISSN - 1097-4555

pISSN - 0377-0486

DOI - 10.1002/jrs.1250240715

Subject(s) - raman spectroscopy , microprobe , diamond anvil cell , fourier transform , infrared , analytical chemistry (journal) , fourier transform infrared spectroscopy , laser , chemistry , raman laser , materials science , optics , mineralogy , raman scattering , diffraction , mathematical analysis , physics , mathematics , chromatography

Near‐IR Fourier transform (FT) Raman spectroscopic measurements were performed at high pressures for the first time by mounting a diamond‐anvil cell on the optical stage of an FT‐Raman microprobe equipped with a long‐range 4 × objective and by using a near‐IR (Nd: YAG, 1064.1 nm) laser to excite the sample. The utility of this new pressure‐tuning Raman microspectroscopic method was demonstrated by its successful application to a typical organometallic complex, Cr(CO) 4 (bipy)(bipy = 2.2′‐bipyridyl), which decomposes under conventional visible Raman spectroscopic conditions.

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