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Crystal standard/metal disc method for the measurement of low‐temperature resonance Raman spectra in the solid state
Author(s) -
Bartholomew C. R.,
McConnell A. A.,
Smith W. E.
Publication year - 1987
Publication title -
journal of raman spectroscopy
Language(s) - English
Resource type - Journals
SCImago Journal Rank - 0.748
H-Index - 110
eISSN - 1097-4555
pISSN - 0377-0486
DOI - 10.1002/jrs.1250180409
Subject(s) - raman spectroscopy , crystal (programming language) , sodium nitrate , analytical chemistry (journal) , metal , spectral line , chemistry , nickel , zinc nitrate , resonance (particle physics) , zinc , single crystal , materials science , inorganic chemistry , crystallography , optics , atomic physics , physics , organic chemistry , chromatography , astronomy , computer science , programming language
Mounting a sodium nitrate crystal on the surface of a disc made by compacting silver powder and the material to be studied enables Raman spectra of compounds such as zinc and nickel phthalocyanine to be measured in such a way that relative peak inteasities in any one disc can be quantified using the nitrate as a standard. It is a good method for the measurement of low‐temperature spectra of resonant compounds and for the measurement of temperature dependence.