Electrospray ionization mass spectrometry study on dipeptide 4‐chlorobutyl ester produced from refluxing of amino acid with phosphoryl chloride in tetrahydrofuran | Zendy

Zhou Gui Ji | Zendy; Liu Ze | Zendy; Wang Tong Jian | Zendy; Xu Peng Xiang | Zendy; Tang Gou | Zendy; Ye Yong | Zendy; Zhao Yu Fen | Zendy

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Electrospray ionization mass spectrometry study on dipeptide 4‐chlorobutyl ester produced from refluxing of amino acid with phosphoryl chloride in tetrahydrofuran

Author(s) -

Zhou Gui Ji,

Liu Ze,

Wang Tong Jian,

Xu Peng Xiang,

Tang Gou,

Ye Yong,

Zhao Yu Fen

Publication year - 2005

Publication title -

journal of mass spectrometry

Language(s) - English

Resource type - Journals

SCImago Journal Rank - 0.475

H-Index - 121

eISSN - 1096-9888

pISSN - 1076-5174

DOI - 10.1002/jms.918

Subject(s) - chemistry , tetrahydrofuran , dipeptide , electrospray ionization , mass spectrometry , chloride , tandem mass spectrometry , electrospray , organic chemistry , fast atom bombardment , lithium chloride , chromatography , peptide , biochemistry , solvent

Phosphoryl chloride was able to promote the formation of peptide and the ringopening of tetrahydrofuran (THF) followed by a sequence of successive reactions by simply refluxing. ESI multistage tandem mass spectrometry was applied to trace the reaction and elucidate the product structures, dipeptide 4‐chlorobutyl ester. Copyright © 2005 John Wiley & Sons, Ltd.

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