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Synthesis of 13 C 1 ‐pinonaldehyde
Author(s) -
Dicus Christopher W.,
Willenbring Dan,
Nantz Michael H.
Publication year - 2005
Publication title -
journal of labelled compounds and radiopharmaceuticals
Language(s) - English
Resource type - Journals
SCImago Journal Rank - 0.432
H-Index - 47
eISSN - 1099-1344
pISSN - 0362-4803
DOI - 10.1002/jlcr.910
Subject(s) - chemistry , ketone , carboxylic acid , lithium (medication) , organic chemistry , endocrinology , medicine
13 C 1 ‐pinonaldehyde is prepared in seven steps from cis ‐pinonic acid. In the key sequence, the introduction of labeled carbon is accomplished by Lieben degradation of a methyl ketone followed by treatment of the resultant carboxylic acid with 13 C‐methyl lithium. Copyright © 2005 John Wiley & Sons, Ltd.
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