Microwave‐enhanced, solvent‐free synthesis of singly and doubly  13 C‐labelled  trans ‐cinnamic acid at the  α ‐ and  β ‐carbon positions | Zendy

Ma Guibin | Zendy; Hayes Sophia E. | Zendy

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Microwave‐enhanced, solvent‐free synthesis of singly and doubly 13 C‐labelled trans ‐cinnamic acid at the α ‐ and β ‐carbon positions

Author(s) -

Ma Guibin,

Hayes Sophia E.

Publication year - 2004

Publication title -

journal of labelled compounds and radiopharmaceuticals

Language(s) - English

Resource type - Journals

SCImago Journal Rank - 0.432

H-Index - 47

eISSN - 1099-1344

pISSN - 0362-4803

DOI - 10.1002/jlcr.878

Subject(s) - chemistry , cinnamic acid , benzaldehyde , malonic acid , microwave irradiation , solvent , ammonium acetate , carbon 14 , ammonium , organic chemistry , carbon fibers , medicinal chemistry , nuclear chemistry , catalysis , high performance liquid chromatography , physics , materials science , quantum mechanics , composite number , composite material

13 C‐labelled trans ‐cinnamic acid (3‐phenyl‐2‐propenoic acid) has been synthesized in one step using benzaldehyde‐carbonyl‐ 13 C and malonic acid‐2‐ 13 C in the presence of ammonium acetate under microwave irradiation and solvent‐free conditions. Copyright © 2004 John Wiley & Sons, Ltd.

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