Synthesis of  13 C and  15 N multilabeled 5‐aminolevulinic acid | Zendy

Iida Katsumi | Zendy; Kajiwara Masahiro | Zendy

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Synthesis of 13 C and 15 N multilabeled 5‐aminolevulinic acid

Author(s) -

Iida Katsumi,

Kajiwara Masahiro

Publication year - 2002

Publication title -

journal of labelled compounds and radiopharmaceuticals

Language(s) - English

Resource type - Journals

SCImago Journal Rank - 0.432

H-Index - 47

eISSN - 1099-1344

pISSN - 0362-4803

DOI - 10.1002/jlcr.541

Subject(s) - chemistry , hydrolysis , condensation , phthalic acid , carbon 14 , chloride , phthalic anhydride , medicinal chemistry , glycine , radiochemistry , nuclear chemistry , organic chemistry , catalysis , amino acid , biochemistry , physics , thermodynamics , quantum mechanics

5‐[4‐ 13 C, 15 N]‐ and 5‐[5‐ 13 C, 15 N]Aminolevulinic acid (ALA) were simply synthesized in four steps by the condensation of [1‐ 13 C, 15 N]‐ or [2‐ 13 C, 15 N]glycine, respectively, with phthalic anhydride, followed by conversion to the chloride, coupling reaction with a three‐carbon unit and hydrolysis. Copyright © 2002 John Wiley & Sons, Ltd.

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